ICS5000+高压离子色谱系统

　　ICS-5000+高压离子色谱

　　Thermo Scientific Dionex ICS-5000+ HPIC高压离子色谱：世界上首款毛细管高压、“只加水”离子色谱系统。全新的模块设计具有极大的灵活性、功能更全面，操作更简便，其完美卓越的性能将色谱分析带入一个新的更高境界，分辨率更佳，分析速度更快。通过毛细管系统以及分析系统整合组成的ICS-5000+高压离子色谱系统，能应对未来潜在的挑战以及高级应用，该系统提高了工作效率，扩展了工作能力、提高了色谱性能。

　　主要特点

　　ICS-5000+具有出色的耐压性能，兼容4μm离子色谱柱，极大提升了峰容量，进一步优化了分辨率。支持小粒径色谱柱分离，大大提高了分辨率，结合快速离子色谱柱，分析速度可提升2倍，实现高分辨率、超快速分析

　　绿色理念离子色谱：毛细管色谱模式下，淋洗液发生器可以连续使用18个月，一年仅消耗5.25 L水，极大降低了试剂的消耗。时刻待机功能可节省大量时间，极大提高了分析效率，降低了实验室的日常消耗

　　兼容毛细管、微孔和标准体系，色谱分析更加灵活

　　单系统和双系统的灵活性配置，支持多种检测器。轻松实现多种联用技术——IC×IC (2D-IC)、IC-MS、IC-MS/MS和IC-ICP/MS。支持多通道、多检测方式，支持多维色谱，具有更高的灵敏度

　　世界第一台集生物液相、氨基酸分析、糖分析、反相液相色谱等功能于一身的离子色谱，可完成糖类、氨基酸、抗生素、小分子药物、核酸以及蛋白质、多肽等的分离测定。电导检测器、脉冲积分安培检测器、紫外检测器、荧光检测器、CAD检测器、荧光检测器、质谱检测器自由配置

　　挑战分离极限

　　ICS-5000+ HPIC高压毛细管离子色谱系统采用小粒径的色谱柱(比如4 μm)，在不增加分析时间的情况下提高了色谱分辨率。

　　• 超强的耐高压能力，支持小内径、标准长度(250mm)的色谱柱

　　• 高效的色谱分辨率，提高了复杂样品分析的准确性

　　• 分离效果，超乎想象——在不增加分析时间的情况下，可以分离出先前难以分离的峰

　　通过优化色谱柱内径，支持高流速缩短分析时间，同时保持高分辨率。快速离子色谱柱有着较短的长度、较大的耐压性能和较小粒径的填料等特点，其分析速度要比常规色谱柱快2倍。

　　• 快速分离，增加样品通量

　　• 提高分析效率

　　• 紧急样品的快速结果筛查

　　系统特性：

　　•泵耐压高达6000 psi

　　• 支持多通道分离，兼容毛细管体系，时刻待机，随时进样

　　• 采用标准型或微孔型色谱柱进行第一维色谱分析，毛细管柱进行第二维分析，获取质谱级检出限

　　• 支持包括电导、电化学、紫外可见光吸收、质谱在内的多种检测技术

　　• 解放您的双手——利用去离子水在线电解产生精确浓度的淋洗液

　　• 颜色标记式管路，人性化设计

　　• 降低使用成本：您可以安排更多时间从事其他重要工作，提高生产率

　　• 新型PdH参比电极，重现性极佳，保证不同时间、不同操作者和不同实验室之间结果的一致性

　　• “谱立方”组件，预装式设计，“零”死体积，组件易于配置，具有单独控温区

　　AS-DV全自动样品处理系统

　　精密机械加工，重现性高

　　支持样品在线过滤等样品前处理功能

　　随机取样和重叠进样功能

　　AS-AP全自动智能样品处理系统

　　支持满环、非满环、毛细管模式和微量样品进样

　　具备自动样品震荡“AutoTrayShake”及“Puncture Offset”穿刺侧移功能

　　全自动在线样品制备(稀释、预浓缩、基体消除、柱前衍生)

　　对热不稳定样品可进行温度控制

　　支持在线监测电导和pH功能，智能判断进样与否

　　色谱数据系统

　　Chromeleon® 7.1变色龙软件是蜚声全球的色谱管理软件，也是世界上zei早实现智能化、人性化、安全性、审计追踪及电子签名的软件之一。变色龙软件充分适应操作者windows的操作习惯，利用鼠标拖拽等进行程序编辑。变色龙软件是世界上屈指可数的全面色谱管理系统，能够双向控制来自30多家公司的近300种离子、液相和气相色谱系统及相关部件。

　　D-Library数据库：通过搜索数据库，您可及时分享国外zei新分析成果。

压力范围：

       分析： 0–35 MPa (0–5000 psi)

       毛细管：0–41 MPa (0–6000 psi)

流量范围：

       分析：0.000-10.000 mL / min的流量，增量可设置在0.001mL / min，无需改变泵头

       毛细管：0.001-0.100mL / min的流量，增量可设置在0.0001mL / min，典型的工作范围为5-30μL / min的流量增量

流量准确度：< 0.1%

流量精度：< 0.1%

压力波动：<1%(1.0mL / min)

真空脱气(分析和毛细管)：集成，可选1元泵通道或4通道四元泵

活塞密封清洗：标准，自动操作

RFIC-EG梯度

         分析：0.1-100mM

        毛细管：0.1-200mM

梯度配比准确度和精密度(分析)：±0.5，在2mL / min

尺寸：41×23×56厘米(16×8.75×21.5英寸)

重量SP：20.4公斤(45磅) - DP：24.1(55磅)

更多参数：

Dionex iCS-5000+ 单泵和双泵指标

泵

类型

串联双活塞泵，微处理器控制，稳定冲程，可变流速，具有专利技术的等动力淋洗液预混功能，无需使用阻尼器

结构

泵头及所以接触淋洗液的部件均采用具有化学惰性的PEEK材质，可兼容反相有机溶剂及pH 0-14的溶液

耐压范围：

0–35 MPa (0–5000 psi) (分析型)

0–41 MPa (0-6000 psi) (毛细管型)

流速范围：

分析型：0.000–10.000 mL/min，增幅0.001 mL/min

毛细管型：0.001–0.100 mL/min，zei高可达3.000 mL/min，增幅0.0001 mL/min

流速精度：<0.1%

流速准确度：<0.1%

压力波动：<1% (分析型)；<0.2% (毛细管型，带阻尼器)在10 &micro;L/min, < 1.0% (无阻尼器)典型

加压：无需加压

真空脱气：内置真空脱气，单通道(等度泵)或四通道(四元梯度泵)

活塞密封清洗：标准配置，自动运行

梯度产生方式：四元低压梯度或电解淋洗液在线产生高压梯度

梯度类型：可产生线性、非线性、抛物线等多种形式的梯度

梯度比例精度和准确度：±0.5%

梯度混合：主动梯度混合器(选配)

Pump泵

Type Dual-piston (in series), microprocessor controlled, constant stroke, variable speed, patented Isokinetic Eluent Precompression 

Construction  Chemically inert, metal-free PEEK pump heads and flow path; compatible with aqueous eluents from pH 0–14 and reversed-phase solvents 

Pressure Range  Analytical: 0–35 MPa (0–5000 psi)

                         Capillary: 0–41 MPa (0–6000 psi)

Flow Rate Range  

Analytical: 0.000–10.000 mL/min with settable flow increments at 0.001 mL/min, without changing pump heads 

Capillary: 0.001–0.100 mL/min flow rate and up to 3.000 mL/min for pump priming mL/min with settable flow increments at 0.0001 mL/min, typical working range of 5–30 &micro;L/min

Flow Rate Precision (Analytical and Capillary)   < 0.1%  

Flow Rate Accuracy  < 0.1% 

Pressure Ripple  < 1% at 1.0 mL/min/typical, < 0.2% (with damper) at 10 &micro;L/min, < 1.0% (without damper) typical

Pressure  None required 

Vacuum Degasser (Analytical and Capillary)     Integrated, optional 1 channel for isocratic pump or 4 channel for quaternary pump

Piston Seal Wash Standard, automatic operation

Gradient Formation (Analytical and Capillary)   Quaternary low pressure (analytical only) or electrolytic eluent generation at high pressure 

RFIC-EG梯度：

• 分析：0.1–100 mM

• 毛细管：0.1–200 mM

• 梯度疲惫准确度：±0.5 at 2 mL/min

RFIC-EG Gradients

• Analytical: 0.1–100 mM 

• Capillary: 0.1–200 mM

• Gradient Profiles Any combination of an unlimited number of linear, convex, and concave positive and negative gradient profiles

• Gradient Proportioning Accuracy ±0.5 at 2 mL/min

• and Precision (Analytical Only)

• Gradient Mixing (Analytical Only) Passive mixers for 2 mm and 4 mm i.d. columns, optional

• Eluent Generation (Analytical and Capillary)     Optional eluent generation (RFIC-EG)

• Eluent On/Off Valve Electrically actuated, standard

• Leak Sensor Optical, standard

System Software

• Software Chromeleon Chromatography Data System software, supports Microsoft &reg;  Windows &reg;  7, Windows 

• Vista &reg; , and Windows XP &reg;  operating systems

• Automated Procedure Wizards Standard feature

• System Smart Startup and Shutdown Standard feature

• Application Templates Standard feature

• Automation Support of 3rd Party Instruments   Fully controls over 300 different instruments from more than 30 manufacturers, including GC, HPLC, and MS

• Customizable System Control Panels Standard feature

• Signal Channels Pump pressure

• Data Trending Plots All numerical device parameters

• System Status Virtual Channels Standard feature

• Power Failure Protection Standard feature

• System Trigger Commands and Contitionals    Standard feature

• Daily Audit Trail Standard feature

• Sample Audit Trail Standard feature

• System Calibration Storage Factory, present and previous. Completely user selectable

• Customized Reporting Standard feature with unlimited report workbooks

• GLP Compliance Optional

Physical Specifications

• Power Requirements 90–265 V ac, 47–63 Hz

• Dimensions (h  × w  × d) 41 × 23 × 56 cm (16 × 8.75 × 21.5 in.)

• Weight SP: 20.4 kg (45 lb) — DP: 24.1 (55 lb)

• Flow Path: All polymeric (PEEK), anion or cation configuration11

EG淋洗液自动发生装置

• zei小和zei大分析：0.1–100 mM

• 淋洗液浓度范围毛细管：0.01-200mM

• 流速范围：分析0.0–3.000 mL/min；毛细管：0.001–0.030 mL/min

• 淋洗液类型：分析: KOH, LiOH, NaOH; Carbonate; Carbonate/Bicarbonate; MSA 
                    毛细管: KOH, MSA

• zei大操作压力：分析: Dionex EGC III: 21 MPa (3000 psi); Dionex EGC 500: 35 MPa (5000 psi)
                        毛细管: 35 MPa (5000 psi)

• 有机物zei大浓度：阳离子：不允许有有机溶剂存在；阴离子：能耐受25%的甲醇

• 淋洗液罐的数量：支持两个淋洗液罐的同时使用

• 电源条件：90–265 V ac, 47–63 Hz

• 尺寸(h×w×d) ：41×23 ×56 cm(16×8.75×21.5in.)

• 重量：25 kg(40 lb)(不带选配件下)

Dionex iCS-5000+ eg eluent generator  specifications

Minimum and Maximum Analytical: 0.1–100 mM

Eluent Concentration Capillary: 0.1–200 mM 

Flow Rates  Analytical: 0.1–3.000 mL/min；Capillary: 0.001–0.030 mL/min 

Eluent Types  

Analytical: KOH, LiOH, NaOH; Carbonate; Carbonate/Bicarbonate; MSA 

Capillary: KOH, MSA

Maximum Operating Pressure  

       Analytical: Dionex EGC III: 21 MPa (3000 psi); Dionex EGC 500: 35 MPa (5000 psi)

       Capillary: 35 MPa (5000 psi)

Maximum Solvent Concentration Cations: None

(Analytical and Capillary)  Anions: 25% methanol (KOH, NaOH and LiOH cartridges); None (Carbonate cartridge and EPM)

Gradient Profiles Standard - any combination of an unlimited number of linear, convex and concave positive and negative gradient profiles

Number of Cartridges Supported Two–dual cartridge support

RFIC Eluent Degasser (Analytical only)

Eluent degasser housed in the EG Module

System Software

Software Chromeleon Chromatography Data System software, supports Microsoft Windows 7, Windows Vista, 

and Windows XP operating systems

Automated Procedure Wizards Standard feature

System Smart Startup and Shutdown Standard feature

Application Templates Standard feature

Automation Support of 3rd Party Instruments   Fully controls over 300 different instruments from more than 30 manufacturers, including GC, 

HPLC, and MS

Customizable System Control Panels Standard feature

Signal Channels Eluent concentration

Data Trending Plots Device numerical parameters plotted

System Status Virtual Channels Standard feature

Power Failure Protection Standard feature

System Trigger Commands and Contitionals    Standard feature

Daily Audit Trail Standard feature

Sample Audit Trail Standard feature

Eluent Cartridge  Information Storage Serial number and expiration date

Customized Reporting Standard feature with unlimited report workbooks

GLP Compliance Optional package provides security, modification history, and electronic signatures

Physical Specifications

Power Requirements 90–265 V ac, 47–63 Hz

Dimensions (h  × w  × d) 41 × 23 × 56 cm (16 × 8.75 × 21.5 in.)

Weight 25 kg (40 lb) without optional items

Flow Path All polymeric (PEEK), anion or cation configuration

Dionex iCS-5000+ er eluent regeneration SPeCifiCationS (analytiCal)

Eluents Carbonate and carbonate/bicarbonate combinations up to 20 mM 

MSA up to 34 mM 

Flow Rates  1.00–2.00 mL/min

Continuous Operation with 4 L of Eluent Up to 28 days or 2000 samples, typically

Always on, Always Ready Capable Standard feature

Remains Fully Calibrated for Extended Standard feature, results are traceable to a single calibration

Periods of Time (≤ 28 Days):

System Wellness Consumables usage monitoring for predictive maintenance

Maximum Operating Pressure 21 MPa (3000 psi)

Operating Temperature Range 4–40 °C

Dionex iCS-5000+ DC DeteCtor/ChromatograPhy ComPartment SPeCifiCationS

Dual Temperature Zone Model Upper Zone Temp. Range: 10–40 °C (minimum temperature: ambient -15 °C); 

(maximum temperature: ambient +20 °C) 

Lower Zone Temp. Range: 10–70 °C (minimum temperature: ambient -15 °C)

(maximum temperature: ambient +50 °C)

Temperature Accuracy: ±0.5 °C

Temperature Stability: ±0.2 °C

Temperature Precision: ±0.2 °C

Lower Zone (Analytical)  Injection Valves: Up to two high-pressure valves,either 6- or 10-port, 2-position

Low Pressure Valves: Up to 2 inert, 2- or 3-way

Reaction Coil Heater (RCH): Holds two reaction coils

RCH Temperature Range: 5 °C above upper zone, 80 °C maximum 

AutoPrep Kit: Dual loop for sample preconcentration 

All valves and heater upgradable and field installable 

Automation Manager    Injection Valves: Up to two high-pressure valves, either 6- or 10-port, 2-position

(Optional - Analytical Only) Low Pressure Valves: Up to 2 inert, 2- or 3-way

Reaction Coil Heater (RCH): Holds two reaction coils

RCH Temperature Range: 5 °C above upper zone, 80 °C maximum 

AutoPrep Kit: Dual loop for sample preconcentration 

All valves and heater upgradable and field installable

Capillary IC Cube  One or two IC Cube modules holding the following:

(Optional - but required for Injection Valves: Up to two (one per cube) high-pressure valves, 4-port, 2-position. An optional capillary chemistries) 6-port, 2-position valve is available to support large loop and concentrator applications

EG Degasser 

Column and Guard

Carbonate Removal Device

Capillary Suppressor (See Suppressor section)

IC Cubes and cartridges are customer installable with pre-formed tubing and color-coded labeling

Capillary column heater 15 to 85 °C)

Flow Path Plumbing configurations for 4 mm, 2 mm, and 0.4 mm columns, fully inert, PEEK 

Detectors Any combination of two conductivity or electrochemical detectors, upgradeable and field installable. 

Dual detectors can be operated simultaneously or independently. Optional remote operation up to 3 m from instrument.

Analog Signal Output Two analog output channels, two 24 V relays, 2 TTL Out and 8 TTL In lines, upgradable and field installable, optional Leak Detection Optical leak sensor standard

Application Control Automation Standard. All DC modules come equipped with two switched AC controllers built-in to automate external devices and the ability to control up to six low pressure 2-way or 3-way valves for fluidic automation

Suppression

Non-Suppressed Conductivity Supported - both anion and cation

Suppressor Wear Parts None. No valves, pumps, peristaltic pump tubing, or inline filters required

Chemical Suppression 2 mm and 4 mm anion and cation membrane suppression available

Displacement Chemical Suppression 2 mm and 4 mm anion and cation membrane suppression available

Electrolytic Suppression, Self-Regenerating     0.4 mm (with optional IC Cube) 2 mm and 4 mm anion and cation. Membrane and MonoDisc 

suppression bed types available. Membrane for capillary (0.4 mm) suppressor

Electrolytic Suppression, Self-Regenerating,    0.4 mm (with optional IC Cube) 2 mm and 4 mm anion and cation. Membrane and MonoDisc 

External Water Mode suppression bed types available for 4 mm and 2 mm. Membrane for capillary (0.4 mm) suppressor Salt Converter Available in 2 and 4 mm versions

Dionex AMMS-ICE Available in 9 mm version

Carbonic Acid Removal for Anions Thermo Scientific Dionex ASRS &trade;  300 or Dionex AMMS &trade;  300 plus Dionex CRD 200 and 

CRD 300 for 2 and 4 mm versions, Dionex ACES &trade;  300 plus Dionex CRD 200 (0.4 mm) for capillary suppressors13

Dionex iCS-5000+ DC DeteCtor/ChromatograPhy ComPartment SPeCifiCationS  (CONTINUED)

Suppressors

Suppression Capacities Dionex ASRS 300 (4 mm): 200 μeq/min

Thermo Scientific Dionex CSRS &trade;  300 (4 mm): 110 μeq/min

Dionex ASRS 300 (2 mm): 50 μeq/min

Dionex CSRS 300 (2 mm): 37.5 μeq/min

Dionex AMMS 300 (4 mm): 150 μeq/min

Thermo Scientific Dionex CMMS &trade;  300 (4 mm): 150 μeq/min

Dionex AMMS 300 (2 mm): 37.5 μeq/min

Dionex CMMS 300 (2 mm): 37.5 μeq/min

Dionex AAES: 25 μeq/min

Dionex CAES: 25 μeq/min

Dionex AMMS-ICE 300: N/A

Dionex ACES 300 (0.4 mm): 2 &micro;eq/min

Thermo Scientific Dionex CCES &trade;  300 (0.4 mm): 1.5 &micro;eq/min

Suppressor Void Volumes Dionex SRS 300 (4 mm): < 50 μL

Dionex SRS 300 (2 mm): < 15 μL

Dionex MMS 300 (4 mm): < 50 μL

Dionex MMS 300 (2 mm): < 15 μL

Dionex AMMS-ICE 300 (4 mm): < 50 μL

Dionex AES (Anion or Cation): < 35 μL

Dionex ACES 300 (0.4 mm): < 1.0 &micro;L

Dionex CCES 300 (0.4 mm): < 1.0 &micro;L

System Software

Software Chromeleon Chromatography Data System software, supports Microsoft Windows 7, Windows Vista, 

and Windows XP operating systems

Automated Procedure Wizards 2 mm and 4 mm anion and cation membrane suppression available

Electrolytic Suppression, Self-Regenerating     Standard feature

System Smart Startup and Shutdown Standard feature

Application Templates Standard feature

Automation Support of 3rd Party Instruments   Fully controls over 300 different instruments from more than 30 manufacturers, including GC, HPLC, and MS 

Customizable System Control Panels Standard feature

Signal Channels Detector signals, detector background signals, temperatures

Data Trending Plots All device numerical parameters plotted

System Status Virtual Channels Standard feature

Power Failure Protection Standard feature

System Trigger Commands and Conditionals   Standard feature

Daily Audit Trail Standard feature

Sample Audit Trail Standard feature

System Calibration Storage Factory, present, and previous. Completely user selectable

GLP Compliance Optional

Physical Specifications

Power Requirements 90–265 V ac, 47–63 Hz; (auto-sensing power supply; no manual voltage or frequency 

adjustment required)

Dimensions (h  × w  × d) 44.5 × 42 × 57 cm (17.5 × 16.5 × 22.5 in.)

Weight 38 kg (84 lb) 

Flow Path All polymeric (PEEK), anion or cation configuration14

Dionex iCS-5000+ CD ConDuCtiVity DeteCtor SPeCifiCationS

Electronics Type Microprocessor controlled digital signal processing, autoranging

Cell Drive  8 kHz square wave

Linearity    1%

Resolution  0.00238 nS/cm

Flow Path Plumbing configurations for 4 mm, 2 mm, and 0.4 mm columns, fully inert, PEEK 

Output Range Digital Signal Range: 0–15,000 &micro;S/cm

Analog Signal Range: 0–15,000 &micro;S/cm

Noise, Wet < 0.2 nS at 23 &micro;S/cm background

< 0.1 nS at 1 &micro;S/cm background

Filter Rise times 0 to 10 s, programmable

Sample Rate 1 to 100 Hz, user settable or automatic

Cell Temperature 5 °C above DC upper zone temperature to 60 °C maximum. User settable, working range is

identical to settable range.

Cell Temperature Stability < 0.001 °C

Cell Temperature Compensation Default 1.7% per °C; programmable from 0–3% per °C

Flow Cell Maximum Pressure 10 MPa (1500 psi)

Flow Cell Volume Analytical: 0.7 &micro;L

Capillary: 0.02 &micro;L

Cell Electrodes Passivated 316 stainless steel. Compatible with MSA

Cell Body Chemically inert polymeric material

Heat Exchanger Inert, tortuous-path for low axial dispersion

Software

Software Chromeleon Chromatography Data System software, supports Microsoft Windows 7, Windows Vista, 

and Windows XP operating systems

Automated Procedure Wizards Standard feature

System Smart Startup and Shutdown Standard feature

System Wellness and Predictive Performance  Standard feature

Application Templates Standard feature

Automation Support of 3rd Party Instruments   Fully controls over 300 different instruments from more than 30 manufacturers, including GC, 

HPLC, and MS 

Customizable System Control Panels Standard feature

Signal Channels Conductivity, Total Conductivity

Data Trending Plots Detector numerical parameters plotted 

System Status Virtual Channels Standard feature

Power Failure Protection Standard feature

System Trigger Commands  Standard feature and Conditionals

Daily Audit Trail Standard feature

Sample Audit Trail Standard feature

System Calibration Storage Factory, present, and previous. Completely user selectable.

Customized Reporting Standard feature with unlimited report workbooks

GLP Compliance Optional

Physical Specifications

Dimensions (h  × w  × d) 6.9 × 16.7 × 9.9 cm (2.7 × 6.5 × 3.9 in.)

Weight 400 g (1.6 lb) 15

Dionex iCS-5000+ eD eleCtroChemiCal DeteCtor SPeCifiCationS

Electronics Type Microprocessor controlled digital signal processing

Electronic Noise (Wet Noise) IPAD (Au electrode) < 50 pC at 10 mM KOH, DC Amperometry (GC) < 10 pA at catecholamine eluent

(Analytical and Capillary)

Potential Range -2.0 to 2.0 V in 0.001 V increments

Signal Range (Digital and Analog) Integrated Amperometry: 50 pC to 200 &micro;C

DC Amperometry: 5 pA to 74 &micro;A

Filter 0–10 s response time, user settable

Control Mode Local or remote control using relay closures or TTL, or control using Chromeleon software via DC module

Cell Body Titanium body with narrow-bore PEEK inlet tubing for capillary format, titanium inlet tubing for analytical format. Compatible with 0.2–0.6 mm i.d. columns (PEEK inlet), 2–7 mm i.d. columns (Ti inlet)

Working Electrodes Conventional: gold, glassy carbon, platinum, and silver

Disposable: gold, platinum, carbon, and silver

Reference Electrode pH-Ag/AgCl combination, one piece design (Analytical and Capillary) 

PdH, one piece design (Capillary Only)

Autoranging  Yes

Analog Output User selectable full scale of 10, 100, or 1000 mV

Cell Volume at Working Electrode < 0.2 &micro;L

Maximum Cell Operating Pressure 0.7 MPa (100 psi)

Software

Software Chromeleon Chromatography Data System software, supports Microsoft Windows 7, Windows Vista, and Windows XP operating systems

Detection Modes DC amperometry, pulsed amperometry, and integrated amperometry. Detection modes include use 

of multiple waveforms and multiple integration times to optimize detection conditions for individual 

analytes. Integrated amperometry mode—unlimited changes to the waveform profile&rsquo;s number of segments, duration of each segment, and voltage applied at each segment.

3D Amperometry  Three-dimensional display of the raw integrated amperometry data set, with crosshairs on an (Chromeleon 6.8 software only) isoamperometric plot used to select slices of the plot along the applied voltage axis (to render a chromatogram) and along the time axis (to render a voltammogram).

Automated Procedure Wizards Standard feature

System Smart Startup and Shutdown Standard feature

System Wellness and Predictive Performance  Standard feature

Application Templates Standard feature

Automation Support of 3rd Party Instruments   Fully controls over 300 different instruments from more than 30 manufacturers, including GC, HPLC, and MS

Customizable System Control Panels Standard feature

Signal Channels Electrochemical and total electrochemical signals

Data Trending Plots All detector numerical parameters plotted

System Status Virtual Channels Standard feature

Power Failure Protection Standard feature

System Trigger Commands Standard feature and Conditionals

Daily Audit Trail Standard feature

Sample Audit Trail Standard feature

System Calibration Storage Factory, present, and previous. Completely user selectable.

Customized Reporting Standard feature with unlimited report workbooks

GLP Compliance Optional

Physical Specifications

Dimensions (h  × w  × d) 6.9 × 16.7 × 9.9 cm (2.7 × 6.5 × 3.9 in.)

Weight 400 g (1.6 lb) 16

Dionex iCS-SerieS PDa PhotoDioDe array specifications

Optics

Photodiode Array 1024 element

Pixel Resolution 0.7 nm

Lamps Tungsten and deuterium

Optical Resolution 1.0 nm

Wavelength Range 190–800 nm

Electronics

Analog Outputs Four, 0–3 AU, 1000 mV range

Control Modes Software remote control through Chromeleon software

Flow Cell 

Standard PEEK or SST, 13 &micro;L, 10 mm path length

Semi-Prep PEEK, 0.7 &micro;L, 0.4 mm path length

Maximum Flow Operating Pressure 300 psi (< 2 MPa) PEEK

500 psi (< 3 MPa) SST

Performance

Noise ±10 &micro;AU at 254 nm (flowing water, 2s rise time)

±15 &micro;AU at 520 nm (flowing water, 2s rise time)

Drift < 500 &micro;AU/h

Wavelength Accuracy ±1 nm, self-calibration with deuterium lines, verification with built-in holmium oxide filter

Linearity > 2 AU

Physical Specifications

Power Requirements 90–265 V ac, 47–63 Hz

Operating Temperature Range 4–40 °C (40–104 °F)

Operating Humidity Range 5–95% relative, noncondensing

Dimensions (h  × w  × d) 17.4 × 44.4 × 50.3 cm (6.8 × 17.5 × 19.8 in.)

Weight 18.1 kg (40 lb)

tC thermal ComPartment moDule SPeCifiCationS (analytiCal)

Temperature Range 5–85 °C (max 18 °C below ambient) in 0.1 °C increments

Temperature Performance Accuracy: ± 0.5 °C

Stability:  ± 0.1 °C

Precision:  ± 0.1 °C

Heat up / Cool down Time Typically 15 minutes - 20 °C to 50 °C and 50 °C to 20 °C

High-Pressure Valve Types Six-port/two position - Rheodyne PEEK (injection) valve

Ten-port/two position - Rheodyne PEEK (switching) valve

Column Capacity Three column sets, 1–9 mm

Maximum Column Length 300 mm + 50 mm guard column

Precolumn Heat Exchangers (optional) Two low delay volume exchangers

General Specifications

Standard Chromeleon software

Computer Connection USB

Leak Detection Humidity and vapor sensors

TTL and Relay inputs and outputs Two digital inputs/outputs, two relay outputs

Physical Specifications

Power Requirements 90–265 V ac, 47–63 Hz

Operating Temperature Range 4–40 °C (40–104 °F)

Operating Humidity Range 5–95% relative, noncondensing

Dimensions (h  × w  × d) 17.4 × 44.4 × 50.3 cm (6.8 × 17.5 × 19.8 in.)

Weight 15.4 kg (34 lb)17

Dionex iCS-SerieS Variable waVelength DeteCtor SPeCifiCationS

Optics

Optical System Dual beam forward optics design (monochromator) single or multiple (4-channel) wavelength UV-vis 

detector options 

Light Source Deuterium lamp for UV range; tungsten lamp for visible range

Wavelength Range 190 to 900 nm in 1 nm increments

Electronics

Analog Output Ranges (optional) 0.001–3.0 AU

Rise Time 0.00–4.55 s

Full-Scale Recorder Output 1 V or 10 V

Data Collection rate up to Full dynamic autoranging digital absorbance signal output to Chromeleon software

100 Hz Digital Output

Control Modes Software remote control through Chromeleon software

Flow Cells

Cell PEEK

Cell Path Length 10 mm (Standard and Capillary), 7 mm (Micro)

Cell Volume 11 &micro;L (Standard) 2.5 μL (Micro) 0.18 μL (Capillary)

Heat Exchanger Volume 8.8 &micro;L

Maximum Flow Cell Operating Pressure 725 psi (5 MPa)

Performance

Wavelength Accuracy ±1 nm

Linearity > 2 AU

Bandwidth  6 nm at 254 nm

Noise Typically - < ±2.5 × &micro;AU at 254 nm

Drift < 0.1 m &micro;AU/h at 254 nm

Physical Specifications

Power Requirements 85–265 V ac, 47–63 Hz

Operating Temperature Range 10–35 °C (50–95 °F)

Operating Humidity Range 5–80% relative, noncondensing

Dimensions (h  × w  × d) 15.2 × 44.4 × 50.3 cm (6.0 × 17.5 × 19.8 in.)

Weight 15.4 kg (34 lb)18

Dionex aS-aP autoSamPler SPeCifiCationS

Sample Capacity 10 mL vials: 81

1.5 mL vials: 120

0.3 mL vials: 120

Well Plates: 288 (3 × 96 standard or deep well)

Well Plates: 1152 (3 × 384 standard well) 

Minimum Sample Volume 10 &micro;L can be sampled from a 300 &micro;L microvial; 20 &micro;L can be sampled from a 500 &micro;L microvial

Maximum Injection Volume 7500 &micro;L

Variable Volume Range 1–100 &micro;L in 0.1 &micro;L increments; 100–7500 &micro;L in 1 &micro;L increments

Injection Cycle Time (including sample 15 s with sample overlap function; 30 s for a 5 &micro;L full loop without sample overlap

   prep such as dilution)

Injection Modes Full Loop; Partial Loop; Limited Sample; Capillary

Sampling Technique Pull Mode; Push Mode

Injection Precision Fixed Loop: < 0.3% RSD at 20 &micro;L; Partial Loop: < 0.5% RSD at 20 &micro;L

Capillary Mode: < 0.5% RSD at 0.4 &micro;L

Dilution 1:1 to 1:1000

AutoDilution With post-run functionality and Chromeleon AutoDilution License

Dilution Precision < 1.0% RSD for a 1:10 dilution

Carryover < 0.01% with 500 &micro;L flush volume

Sample Tray Thermostatting 4 °C to 60 °C, optional

Sample Conductivity and pH Inline measurement of sample conductivity and pH with postrun functionality, optional

Dual Instrument Support Sequential (asynchronous) and Simultaneous modes, field upgradeable, optional

Sample Degassing CRD 200/300, upgradeable, user installable

Injection Valves One or two 2-position, 6- or 10-port

Diverter Valve One 2-position, 6- or 10-port

Sample Preparation Dilution, addition of internal standards, concentration/matrix elimination, derivatization, etc.

Inline Sample Filtration Dual filter, backflush, optional

Software

Software Chromeleon Chromatography Data System software, supports Microsoft Windows 7, Windows Vista, 

and Windows XP operating systems

Automated Procedure Wizards Standard feature

System Smart Startup and Shutdown Standard feature

System Wellness and Predictive Performance  Standard feature

Application Templates Standard feature

Automation Support of 3rd Party Instruments   Fully controls over 300 different instruments from more than 30 manufacturers, including GC, HPLC, and MS

Customizable System Control Panels Standard feature

Power Failure Protection Standard feature

System Trigger Commands Standard feature and Conditionals

Daily Audit Trail Standard feature

Sample Audit Trail Standard feature

System Calibration Storage Factory, present, and previous. Completely user selectable.

Customized Reporting Standard feature with unlimited report workbooks

GLP Compliance Optional

Physical Specifications

Dimensions (h  × w  × d) 44.5 × 35.9 × 51.6 cm (17.5 × 14.1 × 20.3 in.)

Weight < 25.2 kg (< 55.5 lb)

< 26.8 kg (< 59.0 lb) with sample temperature control

Power 90–265 V ac, 47–63 Hz

Flow Path All polymeric (PEEK), anion or cation configurations